30 August 2026 to 3 September 2026
Europe/Berlin timezone

The effect of high-pressure induced plasticity on the microstructure and properties of nano-structured transparent ceramics fabricated using high-pressure spark plasma sintering

31 Aug 2026, 14:41
20m
Brüssel Saal (Eurogress Aachen)

Brüssel Saal

Eurogress Aachen

3. Oral presentation Field assisted sintering technology/Spark Plasma Sintering FAST/SPS Field assisted sintering technology/Spark Plasma Sintering FAST/SPS

Speaker

Sandrine COTTRINO (Laboratoire MATEIS - INSA de Lyon)

Description

Transparent ceramics have great potential for applications in lasers, optical systems, armor and nuclear technologies. Magnesium aluminate spinel is a promising transparent ceramic that can be prepared by conventional multi-stage processes. However, single-stage spark plasma sintering (SPS) is a less time-consuming approach. Polycrystalline alumina is another widely used engineering ceramic. However, α-Al2O3 is birefringent (hexagonal crystal structure). Hence, high transparency in the visible domain can be only obtained with very low residual porosity (< 0.1%) and grain sizes smaller than the incident light wavelength to limit scattering losses. In this work, high-density nanostructured MgAl₂O₄ and α-Al2O3 ceramics were produced by high pressure SPS (HP-SPS) up to 5 GPa. High pressure densification produces green bodies with fine pores and high density, which improves the sintering process. In fact, application of 1.5 GPa pressure reduces significantly sintering temperatures (< 1000°C), resulting in dense, transparent ceramics without grain coarsening. It has been shown that high pressures induce not only high green density but also plasticity within the ceramic nanoparticles. The objective is to understand how this plasticity modifies the sintering mechanism and affects the final properties. Advanced analysis techniques have been used to monitor microstructure evolution and properties under high pressure and temperature (SEM, TEM, Real in line transmission, Hardness tests).

Professional Status of the Speaker Senior Scientist
Invitation letter for visa No
Interest in submitting a paper in a special issue of Journal of the European Ceramic Society (Elsevier)

Author

Sandrine COTTRINO (Laboratoire MATEIS - INSA de Lyon)

Co-authors

Alexandre Maître (IRCER, UMR CNRS 7315, Univ. Limoges, F-87068 Limoges, FRANCE) Prof. Laurent Gremillard (Laboratoire MATEIS - INSA de Lyon) Marion Vandenhende (IRCER, UMR CNRS 7315, Univ. Limoges, F-87068 Limoges, FRANCE) Dr Nicholas Blanchard (ILM, Université Lyon1-CNRS, UMR 5306, Université de Lyon, 69622 Villeurbanne, France) Pascal Munsh (Université Toulouse III Paul Sabatier, CNRS, IRAP, UMR 5277, 31062 Toulouse, France) Rémy Boulesteix (IRCER, UMR CNRS 7315, Univ. Limoges, F-87068 Limoges, FRANCE) Prof. Sylvain Meille (Laboratoire MATEIS - INSA de Lyon) Dr Sylvie Le Floch (ILM, Université Lyon1-CNRS, UMR 5306, Université de Lyon, 69622 Villeurbanne, France) Dr Thierry Douillard (Laboratoire MATEIS - INSA de Lyon) Yann Le Godec (IMPMC, Sorbonne université, Paris)

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